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Adsorption of Phenol Using Hydrochar Modified Layered Double Hydroxide – Kinetic, Isotherm, and Regeneration Studies
 
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1
Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Sriwijaya,, Indonesia
 
2
Graduate School of Mathematics and Natural Sciences, Faculty of Mathematics and Natural Sciences, Universitas Sriwijaya, Indonesia
 
3
Research Center of Inorganic Materials and Coordination Complexes, Faculty of Mathematics and Natural Sciences, Universitas Sriwijaya, Indonesia
 
 
Corresponding author
Aldes Lesbani   

Graduate School of Mathematics and Natural Sciences, Faculty of Mathematics and Natural Sciences, Universitas Sriwijaya, Indonesia
 
 
Ecol. Eng. Environ. Technol. 2023; 5:275-281
 
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ABSTRACT
In this work, hydrochar using to modified nickel aluminum layered double hydroxide (hydrochar@NiAl LDH). The collected data by XRD indicate that 2θ of material at 11.38°, 22.90°, 35.20°, and 61.60°. The FTIR spectrum of hydrochar@NiAl LDH at wavenumber 3448, 1650, 1500-1600, 1348, 1056, and 500-800 cm-1. NiAl LDH and hydrochar have surface areas of 3.288 m2/g and 7.366 m2/g, respectively. The precursors enhance the composite's surface area by 11.879 m2/g. NiAl LDH, hydrochar, and hydrochar@NiAl LDH have optimal pH values of 3, 6, and 6 respectively. The adsorption process is determined by the kinetic model of pseudo-second order and the model of Freundlich isotherm. NiAl LDH, hydrochar, and hydrochar@NiAl LDH had respective maximum adsorption capacities of 25.445, 21.008, and 25.773 mg/g. The increase in regeneration cycles decreases the percentage of adsorbed.
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